X-ray mask and method for providing same

ABSTRACT

The present invention describes a method for fabricating an x-ray mask tool which can achieve pattern features having lateral dimension of less than 1 micron. The process uses a thin photoresist and a standard lithographic mask to transfer an trace image pattern in the surface of a silicon wafer by exposing and developing the resist. The exposed portion of the silicon substrate is then anisotropically etched to provide an etched image of the trace image pattern consisting of a series of channels in the silicon having a high depth-to-width aspect ratio. These channels are then filled by depositing a metal such as gold to provide an inverse image of the trace image and thereby providing a robust x-ray mask tool.

[0001] The United States Government has rights in this inventionpursuant to Contract No. DE-AC04-94AL85000 between the United StatesDepartment of Energy and Sandia Corporation, for the operation of theSandia National Laboratories.

BACKGROUND OF THE INVENTION

[0002] 1. Field of the Invention

[0003] The present invention relates to contact lithographic maskshaving submicron features, and to a method for producing such masks.These tools are useful in the preparation of plating molds forfabricating metal microparts and are particularly useful for providingmolds having lateral feature dimensions on the order of tenths tohundredths of microns while also having feature depth dimensions on theorder of ten to hundred times those dimensions.

[0004] 2. Description of Related Art

[0005] A variety of methods are presently known for making microparts.U.S. Pat. No. 5,256,360 to Li, teaches the use of a precisely controlledmicro-electrode discharge machine (EDM) to make the micro-filter moldand suggests the use of laser-beam micro-machining, or electron-beammicro-machining, as suitable alternative processes. However, Li ('360),also teaches that molds made using conventional integrated circuits (IC)processing and lithographic processes in silicon tend to incorporatehigh internal strain, are prone to damage, are expensive to produce, andthus not economical to manufacture.

[0006] U.S. Pat. No. 5,501,893 to Laermer, et al. describes alithographic technique for etching silicon, generally referred to as“anisotropic etching,” where it is possible to achieve deeply-extendingtrenches while simultaneously providing side walls which are as nearlyparallel and vertical as desired. In order to achieve these geometriesit is necessary to allow etching to progress only on the bottom of theetched trench in the silicon substrate and not on the walls of thetrench. In particular, Laermer ('893) teaches a two stage process foralternately etching an exposed silicon surface in a reactive ion plasmafollowed by coating the etched surfaces with a thin polymerized layer,wherein the polymer coating serves to protect the wall surfaces of thetrench from action of the plasma since these surfaces are not directlyface the incoming flux of plasma ions. However, the polymer layerapplied to the “floor” surface of the trench quickly breaks down in thepresence of the ion bombardment since this surface directly faces theincoming ions. The polymer layer, therefore, forms a very effectiveetching “stop” on those edges or surfaces not directly in the path ofthe ion flux allowing for directional etching.

[0007] The process continues in this manner, alternating etching stepswith coating steps, until the predetermined etching depth of thestructures in the silicon substrate is reached.

SUMMARY OF THE INVENTION

[0008] Therefore, it is an object of the present invention to provide aprocess for fabricating highly accurate, three dimensional x-ray maskingtools.

[0009] It is another object to provide an x-ray mask comprising asilicon substrate having a foil-like metal pattern embedded into thethickness of the substrate.

[0010] Yet another object of the invention is to provide an x-ray maskhaving an embedded metal pattern whose thickness is sufficient toattenuate virtually all x-ray radiation having an energy at or below 10KeV which strikes the pattern in a direction parallel to the metalthickness.

[0011] It is another object of the invention to provide an x-ray maskwherein the embedded pattern comprises a plurality of structuralelements exhibiting features having lateral dimensions of much less than1 micron.

[0012] Still another object of the invention is to provide an x-ray maskwherein the features include both the structural elements comprising thepattern, and the separation distances between those elements.

[0013] Yet another object of the invention is to provide an embeddedpattern having features exhibiting a height-to-width aspect ratio ofgreater than about 30-to-1.

[0014] Another object of the invention is to provide a robust x-ray masktool which is capable of withstanding repeated handling and very longexposure to high-dose x-ray radiation.

BRIEF DESCRIPTION OF THE DRAWINGS

[0015]FIG. 1A shows the first step in an embodiment of the presentmethod wherein a silicon substrate wafer, or the like, is provided.

[0016]FIG. 1B illustrates the application of a photoresist film onto atop surface of the substrate wafer.

[0017]FIG. 1C shows the placement of a negative(positive) trace image ofa desired pattern on the photoresist.

[0018]FIG. 1D a shows the exposure of the uncovered portions of thephotoresist film to a source of radiation in order to transfer apositive(negative) image of the trace image into the photoresist.

[0019]FIG. 1E shows the silicon substrate after portions of thephotoresist layer are developed and removed thereby exposing portions ofsilicon substrate.

[0020]FIG. 2A illustrates the silicon substrate covered by the developedphotoresist in which exposed portions of the substrate are subjected toan etching plasma.

[0021]FIG. 2B illustrates the silicon substrate covered by the developedphotoresist after the exposed portions of the substrate have been deeplyetched.

[0022]FIG. 3A shows the etched silicon substrate, wherein the remainingphotoresist is removed.

[0023]FIG. 3B shows the silicon substrate wherein layers of chromium andof gold are vapor deposited such that the entire top surface of thesubstrate, those portions which are etched and those which are not, iscoated with a thin layer of these metals.

[0024]FIG. 3C shows the metal coated silicon substrate having a secondthicker layer of gold is deposited such that the etched portions on thesubstrate are completely filled onto the thin chrome/gold layer of FIG.3B.

[0025]FIG. 4 shows the removal of the excess thick gold layer from thetop surface of the silicon substrate by planarizing that surface untilthe silicon substrate is again exposed.

[0026]FIG. 5 shows the step in which the back surface across a regionbeneath the gold pattern is thinned by a blanket etch process until thethickness of the wafer beneath the gold pattern is reduced to less thanabout 100 microns and thereby providing the final mask embodiment.

DETAILED DESCRIPTION OF THE INVENTION

[0027] The present invention provides a process for fabricating a robustx-ray mask tool. In particular, the present invention provides a processfor fabricating an x-ray mask tool capable of replicating featureshaving lateral dimension of less then 1 micron. Such a mask has greatutility for production of metal and ceramic microparts by the well-knownLIGA processes since current technology is limited to providing partmolds having lateral features sizes greater then 1 micron.

[0028] Lithographic masks are available with features less then 1 micronand are fabricated typically in 1000 Å chromium supported on glassslips. However, in order for a mask to effectively stop the high energy,high fluence synchrotron radiation used to prepare molds for LIGAmicroparts, the image-stop layer, opaque to x-rays, would need to beseveral microns thick. Typically, LIGA x-ray masks have a goldimage-stop layer at least 8 microns thick. Masks this thick are verydifficult to produce by conventional means if this layer includesfeatures of less than 1 micron across.

[0029] The instant invention employs a combination of processes toproduce a patterned mask which overcomes this limitation. A mask patternis replicated in a thin layer of photoresist applied to a siliconsubstrate, developed to expose the pattern on the surface of thesilicon, the exposed areas deeply etched by a reactive plasma techniqueto provide a series of trenches on the silicon surface, the trenchesfilled by plating a metal opaque to high energy x-rays, the platedsurface planarized, and the substrate thinned to provide the desiredmask.

[0030] General Description

[0031] This invention describes a lithographic mask having x-rayattenuating structures embedded in an essentially x-ray transparentsupport media. Furthermore, the invention describes a lithographic maskhaving features which can have lateral dimensions much smaller than 1micron across, whether those features are the x-ray blocking structuresthemselves or the separation spaces between such structures.

[0032] The process begins with a standard silicon substrate. A layer ofa polymer photoresist is placed onto a top surface of substrate suchthat the layer is no more than 1-2 microns thick. Any technique forapplying such layers may be used, including dipping, spraying, spinningor vapor depositing, and either organic or inorganic resists may beused. The method of application and composition of the resist is notcritical except for the need for providing a coating layer of less than2 microns.

[0033] The resist layer is baked, or otherwise cured, and the desiredimage pattern rendered onto the layer top surface by using any of anumber of conventional lithographic processes, such as by a directcontact transmission mask. It is also possible to create the desiredpattern by imaging the reflection of a non-contact mask through cameraoptics onto the resist surface, or by directly “writing” the image byusing a programmable e-beam writer. Important to the proper operation ofthe invention is the ability of the exposing “light” used to penetratethe full depth the resist since it is known that as “light” wavelengthsdecrease toward the hard UV (<190 nm) their penetrating power issignificantly reduced necessitating thinner resist layers. Being able tofully penetrate the resist layer will allow the user to achieve the verysmall lateral dimensions desired. Use of a thin resist layer and abroadband light source helps to satisfy this requirement.

[0034] Since the resist coating will act as an etchant barrier duringsubsequent processing, the amount of protection needed will bedetermined by the processing necessary to provide the desired structure.Different combinations of resist compounds provide additional options.In the present case a thin polymer resist is placed directly onto asilicon substrate, cured, masked and exposed to broadband light. Such astructure can provide about a 50-to-1 processing-protection ratio; asufficiently robust etchant barrier to allow etching deep, narrow,channel structures in the silicon substrate. A composite resistcomprising a thin layer of conventional polymer resist may be appliedover a thin silicon dioxide layer grown onto the silicon substrate,where UV light is used to create the image pattern. Such resists permitdirect transfer of the image into a silicon dioxide (glass) “hard”resist which provides a processing protection ratio of 200-to-1 which isabout equivalent to the former resist barrier since the glass resistlayer is much thinner, typically about 1000 Å.

[0035] After rendering the image of the mask into the resist, the resistlayer is chemically “developed” and the exposed areas of the resisteither removed or retained, depending upon the specific resist chemistryused.

[0036] Following the development of the resist, the patterned substrateis exposed to a series of anisotropic reactive etching steps such asthose set forth in the so-called BOSCH process described in U.S. Pat.No. 5,501,893, herein incorporated by reference in its entirety. Inthis, or similar anisotropic processes, the top surface of the siliconsubstrate is protected by the retained resist layer. This first etchingstep is followed by a first polymerization step which coats the walls,edges and bases of the etched recesses in the silicon substrate. Plasmareactor parameters and etching times are adjusted and limited to avoidexcessive damage to the resist layer and the process proceeds in thismanner, alternating between etching and coating steps, until a etchdepth of between 10 to 30 microns is achieved. In particular, in orderfor an mask to effectively stop the high energy synchrotron radiationused to prepare molds for LIGA microparts, a thickness of at least 8microns of gold is necessary. Etch depths of at least this dimension aretherefore critical to the success of this invention.

[0037] After etching the silicon substrate, the remaining resist isstripped away and the substrate cleaned, after which a “seed” layer of0.025 microns of chromium followed by 0.08 microns of gold is vapordeposited onto the entire surface. Alternately, this layer may beomitted if the substrate used is a doped, highly conductive, form ofsilicon.

[0038] Where the more conventional undoped silicon substrate is used, asecond, thicker gold layer is deposited over the “seed” layer so as tocompletely fill and cover the etched recesses. Coating is typically doneby electroplating or by electroless deposition onto the “seed” layer butmay be done by any method providing the applied layer is uniform incomposition and structure and provides a continuous, condensed layer.The thick x-ray blocking layer may be laid down, for instance, bycontinuing the vapor deposition of the “seed” layer, by plasma spraying,or by epitaxy deposition. Time and cost, however, favor a platingprocess.

[0039] Once plated, the incipient mask is planarized by lapping the topsurface of the substrate in order to remove the metal layers from thissurface leaving the surface flat, and essentially free of the platedmetal. What remains is a silicon substrate with a fine metal structureembedded into the thickness of the substrate forming an imaging patterncomprising a gold (or other similar x-ray opaque material) “ribbon”structures extending to a depth of 10 microns or more wherein the widthsof the structures may be less than 1 micron is provided

[0040] In a final step, the back surface of the silicon substrate, theside opposite the planarized surface, is etched away in a regionunderneath the plated gold pattern to a depth sufficient to reduce thetotal thickness of the silicon in this region to below about 100microns. This is done because it is known that x-ray radiation at energylevels of about 10 KeV is not significantly attenuated by passingthrough silicon of these thicknesses.

[0041] Specific Description

[0042] An embodiment of the steps of the invention are described withreference to FIGS. 1 through 5.

[0043] As required, detailed embodiments of the present invention aredisclosed herein. However, it is to be understood that the disclosedembodiments are merely exemplary of the present invention which may beembodied in various systems. Therefore, specific details disclosedherein are not to be interpreted as limiting, but rather as a basis forthe claims and as a representative basis for teaching one skilled in theart to variously practice the present invention.

[0044] Referring to FIG. 1A, the process begins with a silicon substrateor wafer 10. This substrate can, generally, having any useful shape andthickness but should of necessity be a thin wafer having parallel topand bottom surfaces 11 and 12. In particular the present invention ismost easily implemented by using an industry standard 100 mm Ø×0.67 mmthick wafer. In FIG. 1B a liquid photoresist film 20 (herein SRP 3612Novolak) is applied by spin coating to a thickness of about 1.8 micronsor less, and then baked at a temperature of 95° C. for about 90 secondsin order to at least partially cure the resist layer. The particularresist thickness is chosen so as to balance the need for providing athick enough layer to protect the unexposed portions of the siliconsubstrate from the effects of the later ion etch phase against thedesire to fully expose the full thickness of the resist during the lightexposure phase.

[0045] In a next step, shown in FIG. 1C, a standard direct-contactlithographic mask 13, herein embodying a negative trace image of thedesired pattern, is placed directly on the surface of the of resistlayer 20 (FIG. 1C intentionally shows mask 13 above this surface forclarity sake only). In FIG. 1D the exposed portions 14, of the resistlayer 20 are subjected to a source (not shown) of broadband light, 15.Mask 13, is itself formed by depositing a 1000 Å-5000 Å thick layer ofchromium, or similar material, into a glass support slip and comprises aplurality of lines and other structures and features, and separationsbetween features, some of which have minimum lateral dimensions(dimensions in the plane of the mask, perpendicular to separate patternfeatures) of less than 1 micron. The resist exposure source used hereinwas a high pressure mercury-vapor lamp emitting light over a spectralrange of about 365 nm to 450 nm and providing a dose of approximately 80millijoules/cm² measured at a wavelength of 365 nm.

[0046] In the next step in the process, illustrated in FIG. 1E, thephotoresist is chemically “developed” and the exposed portions, 14, ofphotoresist layer 20 are removed. What remains are the unexposedportions, 22, of the resist in an inverse image of the mask patternwherein this inverse image comprises “clear” areas 23 of exposedsilicon. Again, this step is performed using standard and well-knownlithographic processes.

[0047] It should be noted that the choice of a positive or negativeimage mask depends largely on the nature of the photoresist used, i.e.,depending upon whether or not the exposed portion of the photoresist isremoved or left intact after the resist has been developed. Eitherapproach is possible, although, depending on the nature of the desiredpattern, one is usually more preferred than the other.

[0048] After cleaning and drying, the patterned substrate 10 issubjected to an anisotropic reactive plasma etching process, shown inFIG. 2A, such as the BOSCH or other similar etch-and-coat technique,wherein the exposed areas 23 of the silicon substrate 10 are etch to adepth d which is substantially greater than the width w of etchedchannels 25. This step provides the very high aspect ratio etchedpattern shown in FIGS. 2B. As noted supra. the BOSCH process is a twostep etch-and-coat process wherein the intervening coating stepcomprises coating the exposed silicon with a thin layer of a polymerfilm 24 which protects the walls and edges of the etched channel but isquickly destroyed on those surfaces which directly face the bombardmentof the reactive plasma 26 shown in FIG. 2A. This action has the effectof etching channels or trenches in the exposed silicon which have asubstantially uniform width and substantially parallel walls. Theprocess continues until the desired etch depth d has been achieved. Inthe case of the present invention the desired depth was 30 microns butany depth, which achieves the stated intent of creating an x-rayblocking mask, is possible.

[0049] After etching the silicon wafer 10 to the desired depth, theremaining resist layer 22 is removed and the part cleaned leavingsubstrate 10 with a pattern of etched surfaces 27 across top surface 11of the wafer. The entire surface is subsequently covered with a thinelectrically conductive metal film 30, as shown in FIG. 3B, inpreparation for a much heavier coating. The chosen process for applyingthe first thin coating of FIG. 3B is a thermal evaporation or particlevapor deposition (PVD) process, although any other coating process whichwould provide a thin, continuous layer of conductive material would beequally effective. However, any such processes must be able to coat boththe walls 28 and the bases 29 of the etched channels 25. Such methodscould include, but are not limited to, sputtering and chemical vapordeposition or spraying coating methods, and only require that thecoating process provide a continuous, adherent, and conductive layer.

[0050] As disclosed herein, the film 30 is about a 250 Å (0.025 microns)layer of chromium with an overlaying layer of about 800 Å (0.08 microns)of gold. Any similar metal or combination of metals would be usefulincluding most of the metals in the Transition series of metal listed inNew IUPAC Group Numbers 4-12 of the Period Table of elements, alloysthereof, and certain of the metals of Groups 13 and 14, such as aluminumand tin.

[0051] Film 30 is necessary to enable adherence of a final, thickermetal layer 31 which is deposited in a subsequent step, shown in FIG.3C. In the present invention, layer 31 is also gold but as before, couldbe any similar metal selected from the list supplied above, providingthat the etch depth d of the mask is adjusted to provide for asufficiently thick layer of metal to effectively block or substantiallyattenuate the aforementioned synchrotron flux while remaining below a100 microns thickness limit known to be about the limit at which siliconis no longer “transparent” to such radiation but will itself begin toattenuate the x-ray beam and thus will begin to degrade to transmissionand resolving power of the x-ray mask.

[0052] Following the final step of depositing the thick x-ray blockinglayer 31, the mask assembly is planarized, as shown in FIG. 4, to removemetal from across top surface 11 of supporting silicon substrate 10, andto provide a planarized surface 32. Planarizing is typically performedby lapping the top surface until the surface of the silicon is reachedleaving only the embedded metal pattern 33 exposed. This is done toremove the “overburden” x-ray blocking metal layer on the top surface ofthe substrate leaving only the metal deposited in etched channels 25.Planarized surface 32 is also intended to be as flat and smooth aspossible since it is the surface which will lay against the surface ofthe material onto which the synchrotron radiation is to be illuminated.

[0053] A final thinning step, illustrated in FIG. 5, is intended toreduce the thickness of silicon substrate 10 across a region 34 beneaththe embedded metal pattern 33. Thinning is performed on the back side 12of wafer 10 using a standard blanket etching techniques until thethickness of silicon everywhere underneath region 34 of the metalpattern 33 is reduced to about less than 100 microns. As explained aboveit is known that silicon is transparent or nearly transparent tosynchrotron radiation of 10 KeV at thicknesses below about 100 microns.

[0054] Finally, because a plurality of metal patterns would be embeddedon each silicon wafer, the thinning step is most easily performed byreducing the thickness of the wafer across the entire surface underwhich such patterns have been created. Doing so however, will inevitablyweaken the wafer to the point where it cannot be manually handled. Insuch cases, unetched areas in the form of struts spanning the diameterof the wafer are allowed to remain as strengthening members.

[0055] At this point, the x-ray mask is complete. By implementing thesesteps, a mask having blocking structures with lateral dimensions of lessthan 1 micron are achievable. The mask is utilized by placing itsplanarized surface 32 directly onto the surface of the article which isto be exposed to the synchrotron radiation, and illuminating thisassembly with the radiation.

[0056] The foregoing description of the invention has been presented forpurposes of illustration and description and is not intended to beexhaustive or to limit the invention to the precise form disclosed. Manymodifications and variations are possible in light of the aboveteaching. The embodiments were chosen and described to best explain theprinciples of the invention and its practical application to therebyenable others skilled in the art to best use the invention in variousembodiments and with various modifications suited to the particular usecontemplated. The scope of the invention is to be defined by thefollowing claims.

What is claimed is:
 1. An x-ray mask tool, comprising: a siliconsubstrate having a thickness and a top surface and a bottom surfacessubstantially parallel to said top surface, said substrate having atleast one pattern etched into said top surface, said pattern extendingto a depth into said thickness, said pattern comprising a plurality ofetched channels having substantially parallel sides, said channelsfilled with a metal deposit such that said metal deposit is flush withsaid top surface, said pattern further comprising features havinglateral dimensions of less than 1 micron.
 2. The x-ray mask tool ofclaim 1, wherein said metal deposit is any metal capable of attenuatingx-ray radiation to an energy of below about 0.1 KeV in a distance ofless than about 100 microns.
 3. The x-ray mask tool of claim 1, whereinsaid metal deposit is a metal selected from the group consisting of theTransition series of metals listed in New IUPAC Group Numbers 4-12 ofthe Period Table of elements, aluminum, tin, and alloys thereof.
 4. Thex-ray mask tool of claim 1, wherein said metal deposit consistsessentially of gold.
 5. The x-ray mask tool of claim 3, wherein saidmetal deposit comprises a thin vapor deposited first metal layer.
 6. Thex-ray mask tool of claim 5, wherein said vapor deposited first metallayer comprises a first layer of chromium.
 7. The x-ray mask tool ofclaim 5, wherein said metal deposit is deposited by electroplating. 8.The x-ray mask tool of claim 5, wherein said metal deposit is depositedby electroless deposition.
 9. The x-ray mask tool of claim 5, whereinsaid metal deposit is deposited by thermal or particle vapor deposition.10. The x-ray mask tool of claim 5, wherein said metal deposit isdeposited by sputter deposition.
 11. The x-ray mask tool of claim 5,wherein said metal deposit is deposited by molecular beam epitaxy. 12.The x-ray mask tool of claim 1, wherein said silicon substrate isthinned from said bottom surface to a thickness of less than 100 micronsacross a zone encompassing said pattern.
 13. A method for fabricating anx-ray mask tool, comprising the steps of: providing a silicon substrate;forming a first photoresist layer onto a top surface of said substrate;aligning an image patterning mask onto said photoresist layer, whereinsaid mask has portions that block light and portions which transmitlight; exposing said photoresist layer to a source of broadband light;removing said mask; developing said first photoresist layer and removinga portion of said photoresist thereby exposing areas of said siliconsubstrate; anisotropically etching said exposed areas to a depth of atleast about 10 microns providing thereby a plurality of etchedstructures having etched walls and bases; removing the remainingphotoresist; depositing a thin first layer comprising a metal or metalsonto said silicon top surface and onto said etched walls and bases;depositing a thicker second metal layer over said first layer such thatsaid etched structures are completely filled; planarizing said substratetop surface to remove said metal layers from said top surface; andthinning said substrate from a substrate bottom surface in order toachieve a substrate thickness of less than about 100 microns in a regionbeneath said etched structures.
 14. The method of claim 13, wherein thestep of providing a silicon substrate comprises providing a siliconsubstrate that is a standard industry silicon wafer.
 15. The method ofclaim 13, wherein the steps of depositing first and second metal layerincludes depositing a metal selected from the group consisting of theTransition series of metal listed in New IUPAC Group Numbers 4-12 of thePeriod Table of elements, aluminum, tin, and alloys thereof.
 16. Themethod of claim 13, wherein the first step of depositing comprisesdepositing a metal layer by particle or thermal vapor deposition. 17.The method of claim 16, wherein said first step of deposition includesdepositing a layer of chromium followed by depositing a layer of gold.18. The method of claim 13, wherein the second step of depositingcomprises depositing a metal layer by electroplating.
 19. The method ofclaim 13, wherein said second step of deposition includes electroplatinga layer of gold.
 20. The method of claim 13, wherein the step of forminga first photoresist layer onto said substrate comprises spin-coating aNovolak photoresist layer on said substrate.
 21. The method of claim 13,wherein the step of aligning an image patterning mask comprises aligninga positive trace image patterning mask.
 22. The method of claim 13,wherein the step of aligning an image patterning mask comprises aligninga negative trace image patterning mask.
 23. A method for fabricating anx-ray mask tool, comprising the steps of: providing a doped siliconsubstrate, said dopant rendering said substrate electrically conductive;forming a first photoresist layer onto a top surface of said substrate;aligning an image patterning mask onto said photoresist layer, whereinsaid mask has portions that block light and portions which transmitlight; exposing said photoresist layer to a source of broadband light;removing said mask; developing said first photoresist layer and removinga portion of said photoresist thereby exposing areas of said siliconsubstrate; anisotropically etching said exposed areas to a depth of atleast about 10 microns providing thereby a plurality of etchedstructures having etched walls and bases; removing the remainingphotoresist; depositing a thick first layer comprising a metal or metalsonto said silicon top surface and onto said etched walls and bases suchthat said etched structures are completely filled; planarizing saidsubstrate top surface to remove said metal layers from said top surface;and thinning said substrate from a substrate bottom surface in order toachieve a substrate thickness of less than about 100 microns in a regionbeneath said etched structures.